Extraction-Optimization of Hydrogel from Lallemantia Royleana Seeds Through Response Surface Methodology
DOI:
https://doi.org/10.71107/ttas0x69Keywords:
Lallemantia Royleana Seeds, Extraction-Optimization, RSM-BBD methodAbstract
The aim of this study was to evaluate the parameters for the maximum extraction of hydrogel (LRH) from the Lallemantia royleana seeds by Box Behnken Design Response Surface Methodology (BBD-RSM). The influence of different parameters such as pH, temperature, water-to-seed ratio (S/W ratio) and water-to-seed contact-time (S/W time) on LRH yield was evaluated. ANOVA p-values showed that these factors were the most significant constraints of the LRH yield. The Scenarios where the Temperature, Concentration and Time are involved in optimizing the aforementioned parameters were generated in the Construct 2 Design-Expert software, which is also capable of producing 2D and 3D contour maps. The maximum LRH yield of 13.73%, was observed when the seed-to-water ratio, contact period and pH were varied in a controlled manner using the RSM-BBD method. The optimal extraction conditions for the production of LRH were a temp. of extraction of 80 degree celsius, pH of 7, contact time for S/W ratio of five hours and S-W ratio of 1:20. The second order polynomial equations were also discovered to fit better the response under consideration.
Downloads
References
[1] Kaur, P., Agrawal, R., Pfeffer, F. M., Williams, R., & Bohidar, H. B. (2023). Hydrogels in agriculture: Prospects and challenges. Journal of Polymers and the Environment, 31, 3701–3718. https://doi.org/10.1007/s10924-023-02859-1 DOI: https://doi.org/10.1007/s10924-023-02859-1
[2] Erum, A., Tulain, U. R., Maqsood, A., Sidra, Malik, N. S., Rashid, A., & Warraich, L. Z. (2023). Fabrication and comparative appraisal of natural and synthetic polymeric pH responsive nanoparticles for effective delivery of dexlansoprazole. Polymer Bulletin, 80, 9113–9129. https://doi.org/10.1007/s00289-022-04489-4 DOI: https://doi.org/10.1007/s00289-022-04489-4
[3] Hussain, A., Jabeen, N., Yaqoob, A., Zafar, S., Khan, M. U., Ayob, E. A., & Khalifa, M. E. (2025). First-Principles Investigation of Diverse Properties of X2CaTa2O7 (X= Li, Na, K, and Rb) Ruddlesden–Popper Compounds for Photovoltaic Applications. Crystals, 15(3), 228. 10.3390/cryst15030228. DOI: https://doi.org/10.3390/cryst15030228
[4] Hussain, M. A., Bukhari, S. N. A., Ullah, M., & Ashraf, M. U. (2023). Polysaccharide-based hydrogel from seeds of Artemisia vulgaris: Extraction optimization and characterization. Gels, 9(7), Article 525. https://doi.org/10.3390/gels9070525
[5] Bostan, A., Razavi, S. M., & Farhoosh, R. (2010). Optimization of hydrocolloid extraction from wild sage seed (Salvia macrosiphon) using response surface. International Journal of Food Properties, 13(6), 1380-1392. https://doi.org/10.1080/10942910903079242 DOI: https://doi.org/10.1080/10942910903079242
[6] Bukhari, S. N. A., Ali, A., Hussain, M. A., Tayyab, M., Alotaibi, N. F., Elsherif, M. A., ... & Ejaz, H. (2022). Extraction optimization of mucilage from seeds of Mimosa pudica by response surface methodology. Polymers, 14(9), 1904. https://doi.org/10.3390/polym14091904 DOI: https://doi.org/10.3390/polym14091904
[7] Falahati, M. T., & Ghoreishi, S. M. (2019). Preparation of Balangu (Lallemantia royleana) seed mucilage aerogels loaded with paracetamol: Evaluation of drug loading via response surface methodology. The Journal of Supercritical Fluids, 150, 1-10. https://doi.org/10.1016/j.supflu.2019.04.003 DOI: https://doi.org/10.1016/j.supflu.2019.04.003
[8] Han, K.-Y., & Choi, J.-Y. (2016). Optimization for chia seed antioxidative activity of solvent extraction using the response surface methodology. The Korean Journal of Food And Nutrition, 29(2), 228-236. https://doi.org/10.9799/ksfan.2016.29.2.228 DOI: https://doi.org/10.9799/ksfan.2016.29.2.228
[9] Hussain, M. A., Ali, A., Alsahli, T. G., Khan, N., Sharif, A., Haseeb, M. T., ... & Bukhari, S. N. A. (2023). Polysaccharide-Based Hydrogel from Seeds of Artemisia vulgaris: Extraction Optimization by Box–Behnken Design, pH-Responsiveness, and Sustained Drug Release. Gels, 9(7), 525. https://doi.org/10.3390/gels9070525 DOI: https://doi.org/10.3390/gels9070525
[10] Mohammad Amini, A. (2019). Balangu ( Lallemantia royleana ) Seed Gum: Rheology and Functions. In (pp. 183-203). https://doi.org/10.1002/9781119418511.ch7. DOI: https://doi.org/10.1002/9781119418511.ch7
Downloads
Published
Data Availability Statement
Data will be made available on request from corresponding author
License
Copyright (c) 2025 Nadia Khan, Qindeel Fatima, Amna Liaqat, Muhammad Amin (Author)
This work is licensed under a Creative Commons Attribution 4.0 International License.
Most read articles by the same author(s)
- Jehanzaib Ahmed, Nazia Shahana Abbas, Muhammad Amin, Sara Hasan, Arooj Anwaar, Ahmad Shazad Saleemi, Nimra Adil, Amna Liaqat, Investigation of Thermal Stability of Bakelite by Isoconversional Thermal Analysis , Conclusions in Engineering: Articles in Press
- Qurat Ul Ain Yasin , Rabia Sattar, Muhammad Amin, Green Synthesis of Silver Oxide Nanoparticles using Zingiber officinale Extract: Catalytic and Antibacterial Potentials of 2-Phenyl Benzimidazole Derivatives , Conclusions in Engineering: Articles in Press
- Ayesha Ashfaq, Muhammad Tallal, Amna Liaqat, Nadia Khan, Nouman Waheed, Muhammad Amin, Carbon Nitride Nanosheet-based Titanium Dioxide Hybrid Photocatalyst for Organic Effluent Degradation , Conclusions in Engineering: Articles in Press
- Rida Iftikhar, Nazia Shahana Abbas, Muhammad Amin, Sara Hasan, Nimra Adil, Ahmad Shazad Saleemi, Arooj Anwaar, Facile Synthesis and Characterization of Silver Nanoparticles Based Sensors for Colorimetric Detection of Mercury Ions , Conclusions in Engineering: Articles in Press
- Rabia Sattar, Faiza Rani, Muhammad Amin, Nazia Shahana Abbas, Kinetic Analysis of Thermal Degradation of Acrylonitrile Butadiene Styrene (ABS) for its Use in Electrical Appliances , Conclusions in Engineering: Articles in Press
Similar Articles
- Kamal Bashir, Mohamed Mosadag, A Novel Resampling Technique for Imbalanced Classification in Software Defect Prediction by a re-sampling method with filtering , Conclusions in Engineering: Vol. 1 No. 1 (2025): Conclusions in Engineering
- Qurat Ul Ain Yasin , Rabia Sattar, Muhammad Amin, Green Synthesis of Silver Oxide Nanoparticles using Zingiber officinale Extract: Catalytic and Antibacterial Potentials of 2-Phenyl Benzimidazole Derivatives , Conclusions in Engineering: Articles in Press
- Ayesha Saddiqa, Yasir Mehmood, Ammar Alsinai, Muhammad Bilal, Oblique Stagnation Point Flow of Maxwell Trihybrid Nano-Material Over a Stretching Cylinder , Conclusions in Engineering: Articles in Press
- Muniba Yaseen Naz, Suleman Ahmad, Uroosa Hadi, Tayyaba Ghani, Robab Mehmood, Atta Ullah Shah, Mazhar Mehmood, Synthesis, Charecterization and Photocatlytic Application of the Grassy-Free Standing Titanium dioxide Nanotunes (Gfs –TiNts) , Conclusions in Engineering: Vol. 1 No. 1 (2025): Conclusions in Engineering
- Muhammad Bilal, Yasir Mehmood, Tabinda Shaheen, Numerical investigation of Maxwell Hybrid Nanofluid flow with polystyrene oil as base fluid , Conclusions in Engineering: Vol. 1 No. 1 (2025): Conclusions in Engineering
- Muniba Yaseen Naz, Fatima Jamshad, Tayyaba Ghani, Atta Ullah Shah, Uroosa Hadi, Mazhar Mehmood, Suleman Ahmad, Synthesis and Characterization of TiO2-MWCNTs Nanocomposit: A Novel route for the efficient degradation of N, N-Dimethylformamide , Conclusions in Engineering: Vol. 1 No. 1 (2025): Conclusions in Engineering
- Rida Iftikhar, Nazia Shahana Abbas, Muhammad Amin, Sara Hasan, Nimra Adil, Ahmad Shazad Saleemi, Arooj Anwaar, Facile Synthesis and Characterization of Silver Nanoparticles Based Sensors for Colorimetric Detection of Mercury Ions , Conclusions in Engineering: Articles in Press
- Irfan Haider, Imtiaz Ahmad Khan, Fatima Kainat, Hassan Ali Akhter, Hassaan Khalid, Nawishta Jabeen, Ahmad Hussain, Theoretical analysis of power-law nanofluid across extended sheet with thermal-concentration slip and Soret/Dufour effect , Conclusions in Engineering: Vol. 1 No. 1 (2025): Conclusions in Engineering
- Omer Siddig Mustafa Hamza, Magdi Mohamed Eltybe Zumrawi, Hassan Mahmood, Acrylic Copolymer Stabilizer for Cost Optimization of Earthy Road Construction , Conclusions in Engineering: Vol. 1 No. 1 (2025): Conclusions in Engineering
- Mohamed Mosadag, Mohammed Ahmed Mohammed, Kamal Bashir , Amin Mubark Alamin, A Comparative Analysis for the Performance of LFW and ORL Databases in Facial Recognition , Conclusions in Engineering: Vol. 1 No. 1 (2025): Conclusions in Engineering
You may also start an advanced similarity search for this article.